Methods
A functionally graded material (FGM) architecture (W → B4C → Eurofer97) was developed using CSAM, supported by neutronics analysis. Powder blends were engineered with suitable binders to enable deposition of metal matrix composites (MMCs) incorporating shielding materials. Process optimisation focused on balancing deposition efficiency, shielding material retention, and interfacial integrity. Demonstrators were produced in planar and tubular geometries and characterised using detailed microscopy, hardness, and dilatometry. Figure 1 shows the Titomic TKF-1000 CSAM cell at TWI that was used for this study.
Results
Dense, defect-free FGM structures were produced using CSAM, with consistent deposition across all MMC layers and strong adhesion at graded interfaces. Microstructural analysis confirmed near-fully-dense microstructures (<2% porosity) throughout the architecture.
Optimised processing achieved >55% overall deposition efficiency, with shielding material retention exceeding 40% across all MMC compositions, including >98% W retention in Al-W systems. Powder feed and binder selection enabled well-controlled compositional gradients.
Mechanical characterisation showed consistent hardness distributions, with minor reductions (~20%) after heat treatment, while dilatometry confirmed stable, temperature-dependent thermal expansion and improved high-temperature stability.
Small-scale planar (120×75×20mm) and tubular (Ø178×300mm, ~38mm wall) demonstrators validated reproducible processing and integration of ceramics, refractory metals, and steels into a single monolithic graded-Z architecture.
Figure 2 presents a representative micrograph of the as-deposited CSAM small-scale graded-Z shielding demonstrator, illustrating the layer sequence from the substrate to the outer surface. Figure 3 shows representative SEM images of the FGM interfaces, while Figure 4 presents a cross-sectional micrograph of a cold sprayed MMC exhibiting >98% W retention. Figure 5 shows the CSAM small-scale graded-Z shielding demonstrator following post-processing.
Overall, the project progressed beyond proof-of-concept, with MMC and FGM systems achieving MRL 3–4, demonstrating CSAM as a viable route for complex, multi-material fusion shielding components.